JOURNALOFRAREEARTHS
Vol.25,Suppl.,Dec.2007,p.72
　　　　　　　　　　　　　　　　　　　　　　　　　　　　　　　　　　　　
ImprovingCorrosionResistanceofCfΠMgCompositesusingRareEarth
ConversionCoatings
SongMeihui(宋美慧),WangChunyu(王春雨),WuGaohui(武高辉)
(SchoolofMaterialsScienceandEngineering,HarbinInstituteofTechnology,Harbin150001,China)
Abstract:ThesurfaceofcarbonfiberreinforcedMgmatrix(CfΠMg)compositeswasmodifiedbytreatmentofrareearthconversioncoating,andnontoxic,non2pollutionCeconversioncoatingswereprepared.Theeffectofcoatingsoncorro2sionbehaviorsofcompositeswasinvestigatedbyelectrochemicalimpedancespectroscopy(EIS)in3.5%NaClsolution.ThehigherEcorrandcoatings.EISresultsshowedthatthehighervaluesofR2were3,resistanceoc2curedintreatmentcontaining3,thecoatingoftreatmentcontainingCe(NO3)3wasCewasobservedbyscanningelectronmicroscopy(SEM),andcoatingswascharacterizedbyenergydispersivespectrometer(EDS).Themicro2cracks2particleswerecharacteristicsofthesecoatings.
Keywords:CfΠMCrareearthsCLCnumber:TG153　　Documentcode:A　　ArticleID:07)-0072-04
　　Asthemostlightstructurematerials,Mgalloyhasexcellentthermalconductivity,electricalconduc2tivity,electromagneticshieldingeffectivenessandgoodmechanicalproperty,andrecently,itisusedinaero2
spaceandautomotivefields.However,itsapplica2tionisrestrictedbecauseofhighthermalexpansionco2efficientandpoordimensionalstabilityofMgalloys.Carbonfibersreinforcedmagnesium(CfΠMg)compos2itesowntheadvantagesofmatrixalloys,andhavelowexpansion,highdimensionalstability,highspecific
strengthandhighspecificstiffness.ThereforetheyofferapplicationinthemirrorholderofSpaceStation,highprecisionairborneradar,precisenavigationsys2tems,frameandsupporterofopticalmeasurementsys2[5]
tem,andsoon.
However,theCfΠMgcompositesareverysuscep2tibletoelectrochemicalcorrosionduetoactiveMgandthedifferencebetweenthereversiblepotentialsofMgandcarbonfibers.Therefore,thereisatendencyforagalvaniccoupletoformbetweenMgandthereinforce2mentconstituents,whichlimitsapplicationofCfΠMgcomposite.Soitiscrucialtosolvecorrosionproblemforthewidelyapplicationofthismaterial.Rareearthconversioncoatingsareusedtoimprovethecorrosionresistanceoitisnon2toxicand
non2pollution.Theprotectionmethodusedforcompos2
itesisthetypeastheonesdesignedformetal.Inthepreviousstudy,littleattentionhasbeenpaidtoap2plicationforCfΠMgcomposite.Inthispaper,thepro2cessofrareearthconversioncoatingswasintroduced,andthecorrosionresistanceofcoatingsonthesurfaceofCfΠMgcompositeswasinvestigated.
1　Experimental
1.1　Materials
CfΠMgcompositeswereobtainedusingapressureinfiltrationprocess.TheT300carbonfiber(about60%vol)wasusedtoreinforceAZ91DMgalloy.Ta2ble1showsthenominalcompositionsofAZ91DMgalloy.Thecompositesforrareearthconversioncoatingpreparationwerediskswithadiameterof15mm,thelengthwas4mm.Theywerepreparedbyelectronicdischargemachining.
Table1　ChemicalcompositionsofAZ91Dalloy
(%,massfraction)
AlloysAZ91D
ΞReceiveddate:;reviseddate:
Biography:SongMeihui(1981-),Fair,Doctorcandidate
3Correspondingauthor(E2mail:)
SongMHetal.　ImprovingCorrosionResistanceofCfΠMgCompositesusingREConversionCoatings
1.2　Conversioncoatingstreatment
Inpresentwork,therareearthconversioncoatingprocessinvolvedfollowingsteps:Polishingwith1000#abrasivepaper→4#metallographicsandpaperfin2ishgrinding→rinsedwithdistilledwater→rareearthconversioncoatings→rinsedwithdistilledwater→driedintheair.Theparametersofrareearthconver2sioncoatingsadoptedtwotreatmentsasfollows:
No.1,CeCl34.7g?L,Oxidants0.3g?L,pH5,30℃for2h,surfacedensityofCeconversion
coatings7.23mg?cm.
No.2,Ce(NO3)33g?L,3gpH5,30℃forh-2
coatings2..
1.3　Thecorrosionrateofdifferentcoatingsandun2coatingssampleswasevaluatedunderimmersiontest2ingin3.5%NaClsolutionatroomtemperature.Elec2trochemicalmeasurementswereperformedinaflatcell.Intheflatcell,theexposureareaofthesample
was0.785cm.AnAgΠAgClelectrodewasemployedasthereferenceelectrode.Thepotentialofthiselec2trodewithrespecttostandardhydrogenelectrodeis+0.197V,auxiliaryelectrodewasgraphite.Poten2tiodynamicpolarizationmeasurementswereperformedin3.5%NaClsolutioninatmosphericair.Electro2chemicalimpedancespectroscopy(EIS)measurementswereperformedbyapplyingasinusoidalpotentialper2turbationof10mV.Theimpedancespectraweremea2suredwithafrequencysweepfrom100kHzto10mHzinlogarithmicincrement.Allelectrochemicalexperim2entswereperformedafterstabilizationoffreecorrosionpotentialatroomtemperature.
mentinsolutioncontainingCe(NO3)3.Theresultsin2dicatedthattheconversioncoatingsdecreasedthecor2rosionratesofCfΠMgcomposite.
PolarizationcurvesforCfΠMgcomposite,withoutandwithcoatings,wereshowninFig.1.Itwascon2clusionthathighercorrosionpotential(Ecorr)andlow2ercorrosioncurrentdensity(icorr)wereobtainedbyCeconversioncoatings.ThehigherEcorris,thehigheristhematerial′moreover,theicorr,theis′sresistancetoCeimprovedtheeffectively.oftreatmentinsolutionCeCl3wasbetterthanCe(NO3)3.Thisre2sultwassimilartoimmersiontesting.2.1.2　EIS　　InordertostudytheeffectoftheCeconversioncoatingforthecorrosionresistanceofthecomposites,thecorrosionbehaviorofcompositesin315%NaClsolutionwasevaluatedbyEIS.Fig.2showstheNyquistdiagramsforuncoatedsampleandCeconversioncoatingexposedto3.5%NaClsolu2tion.TheNyquistdiagramforuncoatingmaterials
1.4　Microstructure
Themicrostructureofthecoatingwasobservedbyscanningelectronmicroscopy(SEM),andenergydis2persespectroscopy(EDS)wasemployedtoinvestigatecomponentsofcoating.
Fig.1　Polarizationcurvesofuncoatingandcoatings
2　ResultsandDiscussion
2.1　Electrochemicalresults
2.1.1　Corrosionratesandpolarizationcurves　　
CorrosionratesofCfΠMgcomposites,withoutandwithdifferenttreatments,werecalculatedfromexperimen2taldateofimmersionin3.5%NaCthecor2
rosionratewas5.63mgΠm?sforuntreatedsamples,
whileitwasabout3.14mgΠm?sfortreatmentinsolu2
tioncontainingCeCl3,and4.33mgΠm?sfortreat2
Fig.2　Nyquistplotsofuncoatingandcoatingssamples
　　　　　　　　　　　　　　　　　　　　　　　　　　　　　　　JOURNALOFRAREEARTHS,Vol.25,Suppl.,Dec.200774
presentedasemicircle,andcoatingmaterialshassim2
ilarsharpofuncoating,butcoatingsampleshowedhighvaluesofimpedancewhichwerelargerthanthevaluesobtainedwithuncoatingsample.
ThesimulationfittingprocedurewasperformedusingtheequivalentcircuitofFig.3(a)foruncoatingsample,theequivalentcircuitforFig.3(a)inthiscaseconsistsoftheresistanceofsolution(R1),resis2tanceofpolarization(R2)andcapacitance(CPE);
KatyaBrunellietal.suggestedthatcorrosionprod2uctscoulddepositinamicro2crackscoatingandaffecttheimpedancespectrumofthecoating,whentheingwasexposedtocorrosiveandproposedanin(b).In,chromiumcouldbereplacedbyCeconversioncoating,Rsrepresentsolutionresis2tance,RcfrepresentresistanceofCeconversioncoat2ing,CPEisaconstantphaseelementrepresentingtheintactlayer,Cd1isthecapacitanceoftheunderlyingmetalandRpisitspolarizationresistance.Itisdiffi2culttoconfirmthevaluesofelectricalparametersintheequivalentcircuitofcoatingsforcontrastingwithvaluesofuncoating.Accordingly,thesimplecircuitisattemptedtocontrastonthevaluesofequivalentcir2cuit.ThevaluesofR2andCforuncoatingandcoatingarelistedinTable2.TheR2valuesofcoatingsampleishigherthanthoseofuncoatingsample,thisconfirmsthebettercorrosionpropertiesofcoatingobtainedafterimmersiontreatmentforCfΠMgcomposites.Thevalue
-2cm)ofR2fortreatmentcontainingCeCl3(348.9Ω?
islargerthantreatmentcontainingCe(NO3)3(144.9
Ω?cm);itshowselectrochemistrycorrosionishard2ertooccurwithconversioncoatingformedin
inwhichCeCl3wasthemainsalt.Itwasfoundthat,underthesameconditions,thesurfacedensityofcoat2inginthesolutioncontainingCeCl3was7.23
mg?cm,higherthanCe(NO3)3(2.98mg?cm).
2.2　Microstructureandcomponents
Thegoldenyellow2coloredCeconversioncoatingshavebeendepositedonthesurfaceofCfΠMgcompos2ites.SphericalparticleswereinSEMobser2onfΠ,asshownin
,thecoatingshadrevealedthepres2asthemajorconstituentsofthese,asshowninFig.6,andtheyweredistribut2eduniformlythroughoutthecoatings.ThisseemstoindicatethatthecoatingswerecomposedoftheCecompounds(oxideorhydroxide).Theevaporationofwatermoleculescausedshrinkageinvolume,allowingcrackstoform.Obviously,thestressassociatedwithshrinkageincreasedwiththethicknessofthecoatings,largerstressinducedmoreseverecracking.Butmicro2structureofcrackshasnoeffectonimprovementofcorrosionresistanceforcomposite.Furthermore,thereweremoreCe2richedparticles,asshowninFig.7,inprocesscontainingCeCl3thancontainingCe(NO3)3.ItisshownthatCeinthecoatingsplayedthemainroleonimprovingthecorrosionresistanceofCfΠMgcom2
Fig.3　EquivalentcircuitofuncoatingandcoatingssamplesTable2　Parameterofequivalentcircuit
SamplesUncoatedsample
TreatmentcontainingCeCl3
(Ω?cm)17.7217.91
(Ω?μF?cm)(cm-2)
1.76×10-43.23×10-48.68×10-5
TreatmentcontainingCe(NO3)317.55
Fig.4　SurfaceofCeconversioncoatings
(a)TreatmentcontainingCeCl3;(b)TreatmentcontainingCe(NO3)3
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Download Xmodgames from Google Drive if the official link fails to work.&Click here:&Mod features:1.Building Mod--It helps you to build faster.2.Adjust Character Level--Get more levels for better enchantment and potion use.3Teleport/Add Items/Backpack Management in Server.4.TMI (Core Settings & Action Features)-Day/Night Switch：Change Time-Weather Control-Survival/Creative Switch: Change the modes in Game-Item Multiplier x64: The item you get will be multiplied by 64.-Block Breaker: Instantly break the blocks. Whether there are drops depnd on your tool levels. -Invincible: Infinite HP &(only works in single player)&-Super Jump: Jump higher than usual.-Sprint:you can run at high speed &Note： (Dash-glide in the sky still being fixed）-Fly: enables you to fly in survival mode (has to be switched ON before entering local servers by others)&5.Add Item (TMI Select Items)6.Backpack Management--Get direct access to your backpack from Xmodgames. The items there can be disposed of very quickly and even be edited.7.Field of View--Players can use the zooming（sniper）and wide-angle feature &for different purposes like photography, video making, adventure expedition, archery, etc. It also works in server.8.Instantly Spawn Mobs【Android】The Mod is for Android. Please make sure you ROOT your device first.
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Tutorials to Minecraft PE Features:Question A: How to use XMOD for Minecraft PE generallyAnswer:1. Tap ON Xbot to call out the floating window.2. Tap on Xmod to mod the game.3.The mod interface is divided into two parts: Major Features & Specifications4. The left column collects all major types of features. Tap to enter the type of feature.5.The right column shows sub-features or specification under the main feature.Question B: What is TMI?Answer B: Too Many Items (TMI Core Feature) - Feature that Controls of Game MechanicsAdvantages over non-Xmodgames users：1. One click to change Game Mechanics, useful for all Minecrafters.Question C: How to use the Feature： TMIAnswer C:1. Day/Night Switch: Tap to set day or set night time. Notice the sun for the time change.2. Survival/Creative Mode Switch: Tap to change Survival and Creative Mode. You don't have to bother to change it outside in the map menu now.3.Weather Control: Rain/S T Fog: Adjust the slider to change the strength of the weather.Note: Snow only occurs in colder areas like tundra while rain occurs elsewhere.4. Lock Time: Turn it ON, and the flowing of Time will be fixed. The sun or the moon won't move any more. So you can have forever Day/Night Mode ingame and play USHC with friends.Note: In Mods for iOS devices, when 【Lock Time】 is ON, you cannot switch Day/Night anymore. To switch Day/Night, you have to turn Lock Time OFF first.In servers (local ones), Day/Night and Lock Time can be different for different clients using XMG, which means one player can be at Night, the other in daytime when playing together.5.Item Multiplier x64: When turning it ON, every item you get will be multiplied by 64.Question D: What is Character?Answer D:Character- Feature that modifies parameters of the player.Advantages over non-Xmodgames users：1. Gain advantage in PVP & PVE2. Empowered with Superman ability3.Save time playingQuestion E: How to use the Feature： CharacterAnswer E:1a.Level Editor (on Android): Adjust the slider to edit Level from 0 to 2000.1b.Level Multiplier: Adjust the slider to set how many levels you will get when you reach the next level.2.Speed Mode: Sprint/Dash: Adjust to set walking speed.Caution: it can be super fast! Set a value you think will be enjoyable!You can combine this speed mod with Accelerator controlling the panoramic time and personal speed at the same time.Additional Trick of Speed: How to do Bullet time, Slow-motion or Time Freeze in Minecraft PE with Xmodgames:1.Turn on Accelerator in the app. It's located in the XMG "More" Tab.2. Launch MCPE Mod. Set Speed to Dash or sprint.3.Set Accelerator to minus and slow the whole game.4.You'll see the whole game slow down while you run superfast.3.Jump Height: Super Jump: Adjust to set jump height in game.Caution: Beware the height of super jump will cause death from falling. So please turn on Invincible (Unlimited Health) when having fun with it.4.Field of View (FOV): Adjust to Zoom-in like Sniper Mode and Zoom-out to super Wide-Angle. Good for Minecraft Photographers, Archers, Adventures and Architects!5.Fixed View (Bow): When turned ON, the FOV will be fixed. So even if you draw a bow or fly or swim, the FOV will be the same. There won't be animation when you draw a bow. Good for Archer's Shooting Arrows. 6.Invincible: Turn On to enjoy unlimited health in game.Caution: Not working when you are client in local/world server. If you owns the multiplayer server, you still enjoys the feature.7. Block Breaker: Break Blocks in an instant. All blocks is breakable including Bedrocks!Note: Whether you will get the dropped item after breaking a block in game depends on your tool level. For example, you can only mine obsidian when diamond pickaxe. You cannot get this block even with Block Break ON without diamond pickaxe. Likewise, iron pickaxe for diamond ores.8.Fly in Survival Mode: Turn ON and you will be able to fly in survival mode. It's advisable to combine it with Speed and Super Jump to soar in the sky.Question F: What is Backpack?Answer F:Backpack - Feature that Helps you Management your backpack in Survival Mode with ease.Advantages over non-Xmodgames users：1. Useful in clearing up useless blocks2. Local Edit of Items or Blocks owned in single & multiplayer.Question G: How to use the Feature： BackpackAnswer G:1.Tap Backpack in the left column to see the specifications.2.Tap on Item icons (if any) you want to edit or delete3.You can tap on All to select All(No) or Un-select All(Yes)4.Slide to adjust the number you want the selected items to become.5.Tap OK to Confirm.6.Tap Del to delete the blocks you don't wantQuestion H: What is Add Item?Answer H:Add Item - Feature that add any item you want to your backpack in survival mode - Extended from TMI.Advantages over non-Xmodgames users：1. Instantly get rare resources in adventures.2.Hidden Items & Easter Eggs you cannot get in normal game play. Recommended for Builders, Sculptors, Trapmakers, Minecraft Artists, Redstone Fans and Mod Developers.Question I: How to use the Feature： Add ItemAnswer I:1.Tap Add Item in the left column to see the specifications in the right column.2.Tap on the tabs in the right column in lower part to switch between different types of items.NOTE: You can slide the bar to see more tabs. There are altogether 7 tabs now: (Blocks - Ores - Tools - Food - Plants - Dyed - Others -Magic)3.Tap on any icon of the blocks you want. You can choose multiple blocks of different types too.4.Slide to adjust the number you want of the selected items.5. Tap on Add. 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Tap ON it.3.In the right column, Skins and Texture is listed.4.To activate skin, adjust skin slider. To activate texture, turn on Texture Switch.5.Then Exit the game from the background totally.6. Relaunch the mod. The skin and texture will be loaded.Caution: Xmodgames Festival Package for MCPE Mod is bigger than usual. But with more surprise. It's worth it downloading! Recommended: Download with Wifi, VPN or when you are in good network conditions.Enjoy!Credits: Xmodgames Team (for the mod)
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6. TMI is to control Core Settings & Action Features in Game.7.Day/Night Switch Controls Time in Game. Tap on Day to Set Daytime and Night to set Night.8.Survival/Creative Switch Controls Game Mode. Tap on the Tab to switch between two status.9.Weather Control: You can change weather conditions now with weather control sliders. Adjust to set conditions. 10.Lock Time:On both platforms of iOS and Android, an advanced control of time is added. The movement of the Sun and the Moon can be locked so the daytime won't change any more.Note: for iOS users, if you wanna change daytime with Day/Night Switch, please make sure to turn OFF Lock Time first.11.Item Multiplier: With the feature ON, the item you get will be multiplied by 64. Turn it OFF you’ll only get one item at a time.
Features:Character:Level Multiplier (on iOS)/Level Editor (on Android)SpeedJump HeightInvincible Block BreakerFly in Survival ModeInstructions for Activation:Character is to control parameters of player's character (Alex/Steve).Level Multiplier (on iOS): multiplies your level by the number you set as you get into the next level.Level Editor (on Android): allows you to set Level from 0 to 2000.Speed modifies your walking/running speed with different stops.Jump Height modifies your character's jump level. Caution: Be careful not to set it too high without Invincible. Or you'll fall to death.It is very useful to leap through woods or jungles or over mountain cliffs. Invincible: grants you unlimited health. You can’t die and won’t fear anything now!Field of View & Fixed View: These help you adjust Field of View. From Sniper to Wide-Angle.Fixed View is specially designed for Archers. Aiming Animation is removed when Fixed View is ON. Block Breaker: enables you to break any blocks in a flash.
Note: Whether there will be drops of items or blocks after breaking them is decided by your mining tool. E.g. Iron Pickaxe for Diamond & Gold Ores.Fly: in the survival mode, this feature allows you to fly (double tap on jump). You can combine it with Super Jump so you can move around like a Super Hero!
Features:Backpack ManagementAdd ItemsAdd MobTeleportBackpack management is a function for players to arrange or edit items in Backpack in a quick way. You can easily select the item(s) in your backpack to edit or delete.
No longer have to hold on the item icon for 5 secs to throw it away.
Add Item is the TMI branch function to select any items or blocks with the amount you desire. It can be used in multiplayer now!The Tabs in Purple Square represent groups of items. ①Select the icons in the checkbox above. ②Then swipe the scrollbar in white square to define the amount. ③Tap “Add” at the right bottom to continue ④A toast will pop up requesting confirmation. Tap confirm. ⑤Now you get the item you want.
Add Mob is a feature that enables you to spawn multiple creatures of kinds with the amount you desire.
Spawn Mobs is to spawn the creatures in Minecraft instantly. (cannot be used in servers opened by others. E.g. public server)①Tap on Spawn Mobs Tab②Choose the mobs you’d like to add③Select the amount in scrollbar and Add④Confirm and enjoy! Teleport records your current coords and grants you the ability to transport between these set points in one click. Teleport in the current map:①Add Coordinates first (tap and name it)②Tap to switch between saved locations③Saved Coordinates can only be used in the map you set them. If you use them in other maps, you can be stuck for a while. Clear first before resetting the Coords)
MCPE Building Mod, Show Coordinates& Direction and Measure. Demo Video:This Mod helps you spawn blocks in large number in an area. How to Use Building Mod 1.Tap on Build Tab on the left column2.Turn ON Building Switch to activate the mod.3.There are two modes for creating shapes with blocks in the mod:A. Spawn Shape at plB. Spawn Shape by Preset Coordinates.
A.Spawn Shape At Placement1.Tap on a given shape/pattern, then configure the parameters.2.Then pick up a block in your item bar.3.Pay attention to the horinzontal and vertical directions in which you place the block. It affects the shape created greatly.4.We advise you use the feature with other TMI features: Show Coordinates & Show Direction.5.Place the block, and a shape with this material will be spawned instantly! N.B.: Apart from Line, which starts from the position where you place the block, other shapes will be spawned at one block away at the left hand side of the character.
B. Spawn Shape By Preset Coordinates1.Select the shape you like2.Then click on the -> button to further set Coordinates of Origin of the shape.3.Edit the parameters. You may have to refer to your actual Coordinates & direction. So turn ON Show Coordinates & Show Direction in TMI, too.4. Save the edited data.5.Then Place a block/item taken from the item bar and the Shape will spawn at the preset point.
Show Coordinates & Show Directions: 1.Tap on TMI Tab.2.Turn ON these features in TMI.3.Your current Coordinates and the direction you're facing will be shown on the screen.
Measurement of distance:In TMI, we added another feature to measure distance between two points.Place your block for Point A and Point B.1.Tap on TMI Tab.2.Turn ON Measure in TMI.3.You are required to put blocks for Point A and Point B.4. Then the shoutout message will show you the difference of coordinates.5. If you continues to place blocks for multiple measurements, the points will be renewed.
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